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conversion rate and selectivity are affected by mixing and reactor design In most cases, selectivity is reduced by a restricted supply of reagents in and through the lms between the phases However, selectivity can be improved signi cantly by manipulation of the interfacial conditions Mixing design and scale-up are critical to successful performance in manufacturing for these regimes The classi cation system by Doraiswamy and Sharma was treated quantitatively for gas liquid systems by Middleton (1992), as summarized in 11 and Section 13-34 Middleton describes ve regimes instead of four, but in general the classi cations are similar Deviations in the case of homogeneous reactions are more amenable to quantitative analysis and can therefore be developed more completely The same local considerations developed in Section 13-2 for homogeneous reactions apply for heterogeneous reactions where expected overall molar ratios between reactants cannot be maintained.

q j, Conv(t) - QSys,Sen(t)

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In heterogeneous reactions, mass transfer limitations at phase boundaries as well as local mixing limitations may affect the reaction For simple reactions overall reaction rates may be affected and usually decrease, but yield is unaffected given equal degrees of conversion For complex reactions, the selectivity may be decreased, but unlike homogeneous systems, may also be increased under certain circumstances (see Example 13-8a) The other key difference between homogeneous and heterogeneous reactions regarding selectivity is that signi cant selectivity effects can occur in heterogeneous systems at far lower absolute reaction rates because the mass transfer limitations can be very severe In addition, these effects can be subject to considerable magni cation on scale-up to plant operations These effects can be visualized as changing the inherent kR2 /kR1 ratio, as measured by independent determination of the rate constants, to an apparent value caused by mass transfer limitations.

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1 For example, we can improve the statistical signi cance of the measured concentration estimate by increasing the number of samples.

In Section 13-3, examples are used to illustrate the mixing issues that can be signi cant for various types of heterogeneous systems The analysis of deviations from ideal behavior in homogeneous systems applies in many of these cases Homogeneous reactions are more amenable to quantitative analysis and can therefore be developed more completely The extension of the principles to heterogeneous systems will be more qualitative because of the complexity of these systems Heterogeneous systems can in some cases be manipulated to achieve improved yields compared to a homogeneous system with the same reactions There can, therefore, be a great advantage in running under heterogeneous conditions or in some cases to deliberately creating a heterogeneous system for the purpose of improving selectivity See Example 13-8a for an illustration..

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the first to call for censuring Joseph McCarthy and was one of the rare Southerners to support civil rights He had been the vice presidential nominee in 1956 but had lost Now, Dr Irene Till, a staffer working on his subcommittee on antitrust and monopoly, had an idea: A few years earlier, when her husband had gone to fill a prescription for an antibiotic, he had been taken aback by the high price Not only that, but all the alternative antibiotics his doctor suggested sold for exactly the same price How about investigating prescription drug costs In subcommittee hearings that ran off and on from December 1959 until October 1960, Kefauver grilled the top executives of major pharmaceutical companies in front of the public and the press Why did they sell drugs for 179 cents per pill when it cost less than 1.

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